ALS Vacuum Policy and Vacuum Guidelines for Beamlines and Experiment Endstations
Beamline Review Committee
August 22, 1995
(Supersedes LSBL #116)
Abbreviations
BRC - Beamline Review Committee
CDR - Conceptual Design Review
EPS - Equipment Protection System
LCW - Low Conductivity Water
PRT - Participating Research Team
PSS - Personnel Safety Shutter
RGA - Residual Gas Analyzer
RSS - Radiation Safety System
UHV - Ultra-High Vacuum
Front end - Front-end components serve to define a beam aperture
for synchrotron radiation and provide necessary beam on/off, radiation
safety, and vacuum-isolation systems for each beamline for both insertion
device and bending magnet sources. The front end components generally reside
inside the storage ring shielding and physically connect the ring vacuum
chamber to the first valve of the beamline.
1. Introduction
The purpose of this document is to:
1. Explain the ALS vacuum policy and specifications for beamlines and
experiment endstations.
2. Provide guidelines related to ALS vacuum policy to assist in designing
beamlines which are in accordance with ALS vacuum policy.
This document supersedes LSBL-116.
The Advanced Light Source is a third generation synchrotron radiation
source whose beam lifetime depends on the quality of the vacuum in the storage
ring and the connecting beamlines. The storage ring and most of the beamlines
share a common vacuum and are operated under ultra-high-vacuum (UHV) conditions.
All endstations and beamline equipment must be operated so as to avoid contamination
of beamline components, and must include proper safeguards to protect the
storage ring vacuum from an accidental break in the beamline or endstation
vacuum systems.
The primary gas load during operation is due to thermal desorption and
electron/photon induced desorption of contaminants from the interior of
the vacuum vessel and its components. The desorption rates are considerably
higher for hydrocarbon contamination, thus considerable emphasis is placed
on eliminating these sources of contaminants.
All vacuum components in a beamline and endstation must meet the ALS
vacuum specifications. The vacuum design of both beamlines and endstations
must be approved by the ALS Beamline Review Committee (BRC) before vacuum
connections to the storage ring are made. The vacuum design is first checked
during the Beamline Design Review (BDR) held before construction of the
beamline equipment begins. Any deviation from the ALS vacuum specifications
must be approved by the BRC prior to installation of the equipment on the
ALS floor. Any modification that is incorporated into a vacuum assembly
without the written approval of the BRC is done at the user's risk and may
lead to rejection of the whole assembly.
Note: All pressure values described in this document are N2 equivalent
values, i.e., all pressures are measured setting the sensitivity in the
ion gauge controller for N2 gas.
2. Policy and Requirements
2.1 Storage Ring Vacuum
The ALS storage ring vacuum system consists of all-metal, chemically
cleaned, bakeable components. It generally operates at pressures of less
than 2 x 10-10 mbar ( 2 x 10-8 Pa, 1 mbar = 0.76 torr) without beam, and
at pressures of less than 1 x 10-9 mbar (1 x 10-7 Pa) with beam.
2.2 Means Used for
Ensuring the Quality of the Storage Ring Vacuum
The main objective of the ALS vacuum policy is to ensure that the vacuum
connection of any beamline and its associated experiment endstations will
not degrade the quality of the storage ring vacuum. Generally, beamlines
may be separated into two broad categories. The ALS vacuum requirements
differ for each category.
Category 1: UHV beamlines
that share the same vacuum as the storage ring.
Category 2: Non-UHV beamlines
in which the vacuum is completely or partially separated from the front
end components and storage ring vacuum by using either a window or differential
pumping.
For both categories, the storage ring vacuum integrity is ensured by
checking that the following three items meet the requirements described
in detail in Section 2:
a. The base pressure in various parts of the beamline.
b. The contribution of high mass gases to this pressure at appropriate
places as checked by the residual gas spectral analysis (RGA), if and when
required.
c. The vacuum interlocks which protect the storage ring in the event
of accidental vacuum failure.
For non-UHV beamlines, it may also be necessary for users to provide
calculations ensuring that, in case of a vacuum failure, the vacuum interlocks
will adequately protect the ALS vacuum integrity.
All beamline components are required to be manufactured according to
the guidelines described in Section 5 of this
document.
2.3 ALS Vacuum Requirements
This section describes the three requirements that must be met for both
categories of beamlines:
2.3.1 UHV Beamlines
(Category 1)
This category of beamline normally shares the same vacuum as the storage
ring and operates under UHV conditions.
(a) Pressure Requirement
The base pressure in all vacuum components that will be directly exposed
to the storage ring vacuum must be less than 2 x 10-9 mbar (2 x 10-7 Pa)
and it is expected that this pressure requirement will be maintained during
the normal operation. However, during the initial scrubbing period of the
beamline components with synchrotron radiation, an increase in pressure
by an order of magnitude may be allowed, with the exception that at the
storage ring exit port, the pressure must be 2 x 10-9 mbar or less at all
times.
(b) Residual Gas
Analysis (RGA) Requirement
The beamline or the vacuum system must be checked for gas analysis, using
a residual gas analyzer (RGA), before it is opened to the storage ring vacuum.
For beamline qualification, the RGA check is generally done downstream of
the first vacuum isolation valve outside the shielding wall. For experiment
chambers, the test may be done in the chamber itself or in the first beamline
chamber upstream of the experiment system. The RGA used must be sensitive
to a partial pressure of 1 x 10-14 mbar (1 x 10-12 Pa) or less and be capable
of scanning in a range of at least 1-200 atomic mass units (AMU). The RGA
scan must indicate that the sum of the partial pressures of gases having
a mass of 46-and-greater (46 AMU) does not exceed 1 x 10-11 mbar (1 x 10-9
Pa).
All new systems as well as beamlines that have been changed and brought
up to air must be checked to ensure that they meet the above vacuum and
RGA requirements before they are allowed to be opened to the storage ring
vacuum.
However, under certain conditions as determined by the ALS vacuum group,
a waiver for RGA requirements may be provided to a beamline and/or experiment
endstation which normally operate under UHV condition. These conditions
include opening of a beamline vacuum chamber or experiment chamber for minor
changes, such as replacing a burnt ion gauge filament, and changing solid
samples which have similar outgasing characteristics. In all cases, a waiver
will only be granted to vacuum systems which have previously been qualified
at least once for meeting RGA requirements, and have achieved a pressure
below 3.0 x 10-10 mbar (3 x 10-8 Pa) after necessary pumpdown and bakeout.
In any case, it is at the discretion of the ALS Vacuum Group or BRC to
make the decision regarding a waiver.
(c) Vacuum Interlocks
Requirement (Protection in the Event of Vacuum Failure)
The storage ring vacuum is protected from accidental vacuum failures
by fast sensor interlocks in case of catastrophic failure, and by ion gauge
pressure interlocks in the event of a relatively slow leak.
Each beamline has one or two fast sensors. The recommended distance for
the fast sensor to be from the fast valve is 10 m or more, to allow enough
time for the fast valve to close before arrival of the gas wave front in
the event of a vacuum break. The fast sensors are interlocked with the front-end
valves and shutters. The front end contains one or more all-metal isolation
valves, a fast-closing valve, and a pneumatically actuated photon shutter
(which is between the storage ring and the fast valve).
If there is an accidental break in the beamline vacuum system, a fast-response
vacuum sensor will detect the break, and the fast valve will close in less
than 10 ms. This also requires the stored beam on insertion device beamlines
to be dumped to protect the fast valve from being exposed to the large power
of synchrotron radiation. The primary vacuum isolation valve between the
storage ring and the beamline will pneumatically close and seal the ring
vacuum in about 3.5 seconds. The photon shutter located between the storage
ring and the isolation valve will also close. These components are controlled
by the Equipment Protection System (EPS) for the front end and the beamline.
More details related to the EPS are given in ALS
Beamline Design Guide, Rev 2,"PUB-3114.
All vacuum interlocks on beamline components supplied by experimenters
must meet ALS design specifications. The ALS will advise users about vacuum
requirements and interlock procedures for monochromators and endstations.
Generally, these should operate under UHV conditions similar to those of
front ends and the storage ring. Electrical connections between user vacuum
interlocks and front-end components will be made and tested by authorized
ALS staff. Fast sensors should be installed outside of the shielding wall
and downstream of the monochromators in positions approved by the BRC.
For each beamline there must be at least one fast sensor located downstream
of the first isolation valve near the outside of the shield wall. Another
fast sensor may be located upstream of the endstation (a suitable place
would be downstream of an exit slit or any other conductance-limiting component).
The fast sensors are set as follows:
Fast Sensor Set Point: A set point of 1 x 10-5 mbar (1 x 10-3
Pa) protects against catastrophic failure. If the pressure at any sensor
is above this value, the corresponding fast valve/s is triggered, which
simultaneously closes the photon shutter and the isolation valve. On insertion
device beamlines, the stored beam must be dumped to protect the fast valve
from being exposed to the large power of synchrotron radiation, as well
as to protect personnel from bremsstrahlung radiation.
In addition, ion gauges (located on either side of the isolation valve)
are interlocked (using ion gauge controllers at set values) to protect the
storage ring against high pressure due to excessive outgasing, a slow leak,
power failure, etc.
The ion gauge controller interlock set points are such that:
Ion Gauge Controller Set Point: Set at 2 x 10-8 mbar (2 x 10-6
Pa) or lower such that, if the pressure exceeds this value, the isolation
valve upstream of the ion gauge will close and seal. The fast valve may
remain open. The stored electron beam will not be affected.
Please note that the above pressure values set for interlocks are higher
than the normal operating pressures.
If any one of the interlocks is triggered, the isolation valves along
with other shutters will close. They should not be re-opened unless:
1. The pressure in that section is below the pre-approved limit, and
2. The pressure in the front end is below 2 x 10-9 mbar (2 x 10-7 Pa).
If the fast sensor is triggered, the operations coordinator will have
to be contacted before beamline can be brought back on line.
2.3.2 Non-UHV Beamlines
with Vacuum Window/s or a Differential Stage (Category 2)
A beamline downstream from the front end may operate in a helium atmosphere
or oil-free rough vacuum under the following conditions:
i. A window capable of withstanding at least 1 atmosphere pressure isolates
the storage ring vacuum from the beamline vacuum.
ii. A thin window with appropriate interlocks isolates the storage ring
vacuum from the low vacuum side of the beamline.
iii. Efficient differential pumping allows downstream components to
operate at higher pressure without affecting the low vacuum requirement
of the front end.
The design of these devices must be approved by the BRC.
(a) Pressure Requirement
The base pressure in all vacuum components upstream of non-UHV equipment
which is directly exposed to the storage ring vacuum must be less than 2
x 10-9 mbar (less than 2 x 10-7 Pa). This pressure requirement must be met
at all times during the normal operation of the beamline.
However, during the initial scrubbing period of the beamline components
with synchrotron radiation, an increase in pressure by a maximum of an order
of magnitude may be allowed.
The maximum pressure downstream of the vacuum window or differential
stage or conductance limiting component may be of any sub-atmospheric value,
as long as the above condition is always maintained.
(b) Residual Gas
Analysis (RGA) Requirement
The vacuum system is to be tested using a residual gas analyzer (RGA)
upstream of the vacuum window or the differential stage. The RGA used must
be sensitive to a partial pressure of 1 x 10-14 mbar (1 x 10-12 Pa) or less
and be capable of scanning in a range of at least 1-200 atomic mass units
(AMU). The RGA scan must indicate that the sum of the partial pressures
of gases having a mass of 46-and-greater (46 AMU) does not exceed 1 x 10-11
mbar (1 x 10-9 Pa). The RGA scan must be performed by the ALS Vacuum Group
for each new experiment before the isolation valve is opened. For experiments
involving materials of potential hazard, the RGA will be monitored either
continuously or intermittently during operation (at the discretion of the
ALS beamline coordinator and or vacuum group).
(c) Vacuum Interlock
Requirements (Protection in the Event of Vacuum Failure)
The storage ring vacuum is protected from accidental vacuum failures
by fast sensor interlocks in case of catastrophic failure, or by ion gauge
pressure interlock(s) in the event of a relatively slow leak.
For non-UHV beamlines, one fast sensor must be installed and it is recommended
that two be installed. The first must be downstream of the first isolation
valve outside the shield wall. The second sensor should be at a place with
potential vacuum break, such as just upstream of a vacuum isolating window
or differential stages.
All vacuum interlocks on beamline components supplied by experimenters
must meet ALS design specifications. Electrical connections between user
vacuum interlocks and front end components will be made and tested by authorized
ALS staff members.
Both fast sensors and ion gauge controllers are set as follows:
i. Fast Sensor Set Point-If the pressure at any sensor is above
1 x 10-5 mbar (1 x 10-3 Pa), the corresponding fast valve/s is triggered,
which simultaneously closes the photon shutter and the isolation valve.
On insertion device beamlines, the stored beam must be dumped to protect
the fast valve from being exposed to the large power of synchrotron radiation,
as well as to protect personnel from bremsstrahlung radiation.
ii. Ion Gauge Controller Set Point-Set at 2 x 10-8 mbar (2 x
10-6 Pa) or lower on all ion gauge controllers measuring the pressure upstream
of the vacuum isolation window or differential stage. If the pressure exceeds
this value, the isolation valve upstream of the ion gauge will close and
seal. The fast valve will remain open. The storage ring will not be dumped.
Ion gauges located downstream of the window or differential stage may be
set at any value, provided the above conditions are met.
Please note that the above set points for interlocks are considerably
higher than the normal operating pressures.
If any of the interlocks is triggered, the isolation valves and the other
shutters will close and must not be opened unless:
1. The pressure in that section is below the pre-approved limit, and
2. The pressure in the front end is below 2 x 10-9 mbar (2 x 10-7 Pa).
If the fast sensor is triggered, the operations coordinator will have
to be contacted before beamline can be brought back on line.
3. Performance Test
The beamline and/or front end must be checked for compliance with the
three ALS vacuum requirements (Vacuum, RGA scan, and Vacuum Interlocks)
by the ALS Vacuum Group, if:
i. The front end is to be opened to the storage ring for the first time.
ii. The branchline is to be opened to the front end for the first time.
iii. Any part of the beamline is changed or brought up to air and is
ready for re-connection to the storage ring vacuum.
For UHV beamlines, the RGA requirement may be waived under special circumstances.
(When it is decided by the ALS Vacuum Group and/or BRC that checking the
RGA requirement is unnecessary and would not provide information of any
practical use. See Section 2.3.)
4. Review of Vacuum
Design
The vacuum design of each beamline is reviewed by the BRC during a beamline
design review. The experiment group (PRT) must demonstrate that the design
will not degrade the quality of the storage ring vacuum and that it follows
the ALS vacuum policies outlined in this document. The PRT should submit:
i. Beamline assembly drawings or suitable sketches to scale.
ii. A list of vacuum components and materials of construction.
iii. A list of pumps, their specifications, and locations.
iv. Information related to vacuum interlock system.
v. Calculations showing that in case of a vacuum failure, the vacuum
interlock will adequately protect the ALS vacuum integrity.
The PRT must obtain BRC approval before ordering any non-standard, non-UHV
vacuum components and before fabricating any beamline components.
Approval of a PRT beamline design by the ALS Beamline Review Committee
does not allow the PRT group to bypass the performance tests outlined in
Section 3.
5. Vacuum Guidelines
for Beamline and Endstation Experiment Chamber Vacuum Systems
ALS beamlines must have all-metal, hydrocarbon-free front end components.
UHV design criteria must be used for the hardware downstream of the front
end, if the hardware and the front end share a common vacuum. The BRC must
approve any deviations from the requirements in this section.
The following is a partial list of items which will help in developing
a UHV system compatible with ALS requirements. Questions or requests for
additional information should be directed to the BRC or the ALS Vacuum Group.
5.1 Materials
Standard UHV-compatible materials must be used in all beamlines sharing
the same vacuum as the storage ring. The following is a list of materials
that are and are not acceptable for UHV. Any material not listed must be
approved.
Acceptable |
Not Acceptable |
Marginal |
Pure metals:
aluminum
copper (incl. Glidcop)
gold
silver
molybdenum
tungsten
titanium |
Zinc- and cadmium-bearing metals and alloys are not
UHV-compatible. |
Fluoroelastomers
may be allowed in the seat of a gate valve with metal bonnet seals.
These valves are only allowed in the places where there is no chance
for the fluoroelastomer to be exposed to radiation. |
Stainless Steel:
300 series (preferred types are: 304, 316, 321, and 347) |
Organic materials are not permitted unless they are
specifically authorized by the BRC. |
Stainless Steel:
SS containing excessive amounts of sulfur or selenium must be avoided. |
Alloys:
Ampco 18
beryllium copper
inconel 600 or 718
mu-metal
Kovar |
|
|
Ceramics:
Alumina ceramics
sapphire
machinable glass ceramic |
|
|
All components must be inspected and leak-tested after fabrication.
5.2 Bellows
Both welded and formed bellows are allowed, provided they are manufactured
using UHV standards.
Since welded bellows are made of thin stainless steel diaphragms welded
on the inside and outside diameters to form a series of convolutions, proper
UHV techniques are required during manufacturing to avoid trapping of hydrocarbons
or contaminants in the crevices of the convolutions. It is strongly recommended
that the bellows be chemically degreased and baked in vacuum before being
installed in the beamline.
Formed bellows are relatively easy to clean, but must be fabricated for
UHV applications.
5.3 Feedthroughs
Ceramic-to-metal type electrical feedthroughs are allowed for making
electrical connections into the vacuum system. No glass-to-metal feedthroughs
are permitted. Voltages and current carried through the feedthroughs must
not exceed the manufacturer's ratings. External covers and cable restraint
are required to protect against the accidental breaking of ceramics (which
is a major cause of vacuum failure).
Bellows-type mechanical rotary and linear feedthroughs manufactured for
UHV applications are allowed. Feedthroughs with
a single fluoroelastomer seal are not permitted. However, two-stage
differentially pumped feedthroughs with fluoroelastomer seals may be allowed,
with approval by BRC.
5.4 Gauges
Glass ionization gauges are not permitted in
beamlines. Nude ionization gauges
with two independent filaments and controllers with electron bombardment
degassing capability are recommended. It is recommended that the cable connection
to the gauge head be bakeable to 200° C and have an enclosed connector
or cable restraint. Cold cathode, thermocouple, or Vactron gauges may be
allowed, if they meet UHV requirements.
5.5 Vacuum Pumps
Any one or combination of the following primary pumps may be used:
Sputter-ion pumps: Ion pumps (either diode, triode, or differential ion)
are the most reliable pumps for UHV use. Differential ion pumps which contain
both titanium and tantalum filaments are recommended, due to their ability
to pump inert gases.
Titanium sublimation pumps (TSP): TSP, in combination with ion pumps,
are very effective in creating UHV.
Non-evaporable getter (NEG) pumps: NEG pumps are made of UHV-compatible,
active metals which pump by chemisorbing gases.
Cryo pumps: May be used with appropriate isolation valves and interlocks,
which must be approved by the BRC.
Turbomolecular pumps: It is strongly recommended that both the turbo
and the backing pump be oil-free. They must be equipped with appropriate
interlock isolation valves for protection in case of pressure and/or power
failures. The use of a turbo pump as a primary pump in the beamline is discouraged
and must be approved by BRC. A turbo pump system (preferably oil-free) with
appropriate interlocks may be used in the endstation experimental chamber.
Diffusion pumps: These are not permitted due
to their inherent risks of oil contamination.
Roughing Pumps: Only oil-free mechanical pumps
may be used as roughing pumps. Under extreme circumstances where
no alternative exists, an exception may be given by the BRC. During the
initial rough-pumping and/or bake-out of the beamline, turbo pumps, cryo
pumps, sorption pumps and or any other oil-free pumps as approved by the
BRC or Vacuum Group may be used. This is allowed only when the front end
isolation valve is closed. They may also be used at the endstations. When
used at an endstation, a pump must be equipped with appropriate interlock
isolation valves for protection in case of a pressure and/or power failure.
Backing Pumps: It is strongly recommended that
only oil-free mechanical pumps be used as backing pumps. Under
extreme circumstances where no alternative exists, an exception may be given
by the BRC.
The vacuum requirements as outlined in Section 2 must always be satisfied.
5.6 Valves and Flanges
All-metal, bakeable UHV valves, flanges, and seals are acceptable. Flanges
with fluoroelastomer seals are not allowed in the beamline. Metal bonnet
valves with fluoroelastomer seals are not allowed in beamlines where the
seal may be exposed to direct synchrotron radiation. If approved by the
BRC, they may be used in places where radiation exposure is not a problem.
5.7 Fabrication
Fabrication of any component which becomes part of the vacuum environment
of the beamline directly exposed to storage ring vacuum must be done using
UHV compatible materials and following UHV-accepted techniques, including:
Surface Preparation: No machining or polishing operation which might
result in contaminants being embedded in the material should be used. All
tapped holes should be vented.
Machining Lubrication: No cutting lubricant may be used which results
in contamination that cannot be removed by standard cleaning methods. The
use of cutting fluid containing sulfur or silicone compounds is not recommended.
Refer to ALS engineering notes LSME-479 (Light Source Beamlines Vacuum SystemGeneral:
Fabrication, Handling, and Cleaning Parts Before Brazing, Stress-Relief
Annealing, or Preliminary Bake-Out at High Temperatures for Ultra-High Vacuum
Service) and LSME-500B (Light Source Beamlines Vacuum Systems General: Fabrication,
Cleaning, and Certification of Stainless Steel Vacuum Chambers for Weldments
for UHV) for the recommended procedures.
Water Cooled Optics: Vacuum-to-water joints are not permitted in the
ALS beamline vacuum systems, unless there is an intermediate guard vacuum.
Refer to ALS technical note M7184 (Mirror Brazing Technique). Vacuum-to-water
joints must be avoided as much as possible in the users' vacuum chamber
systems.
Chemical Cleaning: All UHV components must be vapor degreased, electropolished,
and/or chemically cleaned before installation in the beamline. Refer to
ALS technical note LSME-421A (Light Source Photon Beam Lines-BNL/NSLS XI
Beamline Mirror System M-Zero Mirror System: General Cleaning and Brazing
Procedures for Furnace-Brazed U.H.V. Parts).
5.8 Assembly of UHV
Components
It is highly recommended that assembly of UHV components take place in
a clean room or in a clean laminar flow hood. There are many sources of
contaminants. The single largest sources during assembly are perspiration,
body oils, hair, perfume, etc. Thus, the use of clean gloves, face masks,
lab coats, and head covers during assembly is recommended.
Lint-free paper or cloth wipes are recommended for use with UHV parts.
Ethanol should be used as a wiping solvent, if necessary.
All UHV components which may get exposed to contaminants should be protected
by clean, oil-free aluminum foil or lint-free paper.
No cadmium-plated, brass, lead, or wood tools should be used during assembly.
If a chamber is to be opened to air and cannot be moved to the clean
room, it is recommended that the chamber be purged continuously with dry
nitrogen gas. A liquid nitrogen source is the best choice to get the quantities
of dry nitrogen required. The ALS will provide such a source.
5.9 Venting
If a UHV chamber is to be vented, dry nitrogen should be used for venting
the system. A pressure relief valve is required in the venting system, especially
to protect view ports from exploding. A safe recommendation for the relief
pressure valve setting is 30 mbar (0.5 psi) above atmosphere (a recommendation
by Varian).
5.10 Leak Checking
and Bakeout
It is highly recommended that the whole system be leak-checked before
going through the thorough bakeout. The recommended temperature for bakeout
of a stainless steel chamber is 200° C. There may be other constraints
which may limit the bakeout temperature to a lower value.
For a system which may give high outgassing loads, it is generally recommended
that a nitrogen bake be done, followed by a vacuum bake. During a nitrogen
bake, dry nitrogen gas from an evaporated liquid nitrogen source is pumped
through the assembly while the components are heated.
References
For further details concerning ultra-high vacuum practice, the user may
consult:
1. Practical Vacuum Techniques, by W.F. Brunner and T.H. Batzer,
published by Krieger, 1974.
2. A User's Guide to Vacuum Technology, by J.F. O'Hanlon, published
by John Wiley & Sons, 1980.
3. High Vacuum Technology: A Practical Guide, by Marsbed H. Hablanian,
published by Marcel Dekker, Inc., New York, 1990.
4. Basic Vacuum Practice, Third Edition, Varian Vacuum Products
Training Department, Varian Associates, 1992.
5. Vacuum Policy for ALS Beamlines and Experimental Systems, by
R.C.C. Perera, K.D. Kennedy, J.R. Meneghetti, LSBL-116
6. Light Source Beamlines Vacuum SystemGeneral: Fabrication,
Handling, and Cleaning Parts Before Brazing, Stress-Relief Annealing,
or Preliminary Bake-Out at High Temperatures for Ultra-High Vacuum Service,
by D. DiGennaro, LSME-479.
7. Light Source Beamlines Vacuum Systems General: Fabrication, Cleaning,
and Certification of Stainless Steel Vacuum Chambers for Weldments for
UHV, by D. DiGennaro, LSME-500B.
8. Mirror Brazing Technique, by D. DiGennaro, M7184.
9. Light Source Photon Beam Lines-BNL/NSLS XI Beamline Mirror System
M-Zero Mirror System: General Cleaning and Brazing Procedures for Furnace-Brazed
U.H.V. Parts, by D. DiGennaro, LSME-421A.
10. ALS
Beamline Design Guide, Rev. 2, PUB-3114.
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